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Each type of GBP polymorph was respectively milled in an oscillatory ball mill (Mixer Mill MM301, Retsch & Co., Germany) at 20 Hz for different times up to 120 min at room temperature. A 0.2 g powder sample was placed in a 25 ml volume stainless steel milling jar containing two 15 mm diameter stainless steel balls
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Both ranitidine hydrochloride form 1 and form 2 were milled separately in an oscillatory ball mill (Mixer Mill MM301, Retsch & Co., Germany) at 30 Hz. A 1 g powder sample was placed in a 25 mL volume stainless steel milling jar containing two 12 mm diameter stainless steel balls.
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